Information card for entry 4308250

Structure parameters

• Formula: Cu6 N12 Na14 O105 Si2 W18
• Calculated formula: Cu6 N12 Na14 O105 Si2 W18
• Title of publication: Characterization and Electrochemical Properties of Molecular Icosanuclear and Bidimensional Hexanuclear Cu(II) Azido Polyoxometalates
• Authors of publication: Céline Pichon; Pierre Mialane; Anne Dolbecq; Jérôme Marrot; Eric Rivière; Bineta Keita; Louis Nadjo; Francis Sécheresse
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 5292 - 5301
• a: 13.1745 ± 0.0009 Å
• b: 18.5992 ± 0.0012 Å
• c: 22.5851 ± 0.0013 Å
• α: 90°
• β: 92.244 ± 0.003°
• γ: 90°
• Cell volume: 5529.9 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0484
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.1203
• Weighted residual factors for all reflections included in the refinement: 0.1372
• Goodness-of-fit parameter for all reflections included in the refinement: 1.23
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No