Information card for entry 4309332

Structure parameters

• Formula: H68 Na10 O34 S20 Sn5 Zn5
• Calculated formula: Na10 O34 S20 Sn5.02 Zn4.98
• Title of publication: Unusual Syntheses, Structures, and Electronic Properties of Compounds Containing Ternary, T3-Type Supertetrahedral M/Sn/S Anions [M5Sn(μ3-S)4(SnS4)4]10- (M = Zn, Co)
• Authors of publication: Christian Zimmermann; Christopher E. Anson; Florian Weigend; Rodolphe Clérac; Stefanie Dehnen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 5686 - 5695
• a: 14.8457 ± 0.001 Å
• b: 14.8772 ± 0.0009 Å
• c: 17.5101 ± 0.0011 Å
• α: 97.402 ± 0.001°
• β: 100.211 ± 0.001°
• γ: 103.956 ± 0.001°
• Cell volume: 3633.6 ± 0.4 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0773
• Residual factor for significantly intense reflections: 0.0551
• Weighted residual factors for significantly intense reflections: 0.1449
• Weighted residual factors for all reflections included in the refinement: 0.1593
• Goodness-of-fit parameter for all reflections included in the refinement: 1.003
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No