Palladium(II) Complexes of Bowls, Pinwheels, Cages, and N,C,N-Pincers of Starburst Ligands 1,3,5-Tris(di-2-pyridylamino)benzene and 2,4,6-Tris(di-2-pyridylamino)-1,3,5-triazene
Authors of publication
Corey Seward; Wen-li Jia; Rui-Yao Wang; Suning Wang
Journal of publication
Inorganic Chemistry
Year of publication
2004
Journal volume
43
Pages of publication
978 - 985
a
10.004 ± 0.002 Å
b
21.863 ± 0.006 Å
c
12.034 ± 0.003 Å
α
90°
β
96.205 ± 0.005°
γ
90°
Cell volume
2616.6 ± 1.1 Å3
Cell temperature
294 ± 2 K
Ambient diffraction temperature
294 ± 2 K
Number of distinct elements
5
Space group number
11
Hermann-Mauguin space group symbol
P 1 21/m 1
Hall space group symbol
-P 2yb
Residual factor for all reflections
0.1473
Residual factor for significantly intense reflections
0.0583
Weighted residual factors for significantly intense reflections
0.1337
Weighted residual factors for all reflections included in the refinement
0.1566
Goodness-of-fit parameter for all reflections included in the refinement
