Information card for entry 4310516

Structure parameters

• Formula: C3.22 H3.3 Cl0.11 N0.49 O0.7 Pd0.16
• Calculated formula: C3.21622 H2.86486 Cl0.108108 N0.486486 O0.702703 Pd0.162162
• Title of publication: Palladium(II) Complexes of Bowls, Pinwheels, Cages, and N,C,N-Pincers of Starburst Ligands 1,3,5-Tris(di-2-pyridylamino)benzene and 2,4,6-Tris(di-2-pyridylamino)-1,3,5-triazene
• Authors of publication: Corey Seward; Wen-li Jia; Rui-Yao Wang; Suning Wang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 978 - 985
• a: 12.611 ± 0.006 Å
• b: 15.569 ± 0.007 Å
• c: 17.267 ± 0.008 Å
• α: 69.253 ± 0.008°
• β: 74.993 ± 0.009°
• γ: 82.484 ± 0.01°
• Cell volume: 3059 ± 2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1261
• Residual factor for significantly intense reflections: 0.0512
• Weighted residual factors for significantly intense reflections: 0.0882
• Weighted residual factors for all reflections included in the refinement: 0.1039
• Goodness-of-fit parameter for all reflections included in the refinement: 0.807
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No