Information card for entry 4310865

Structure parameters

• Formula: C22 H24 Cu N2 O9 Pb
• Calculated formula: C22 H24 Cu N2 O9 Pb
• SMILES: [Pb]1(OC(=O)C)(OC(=[O]1)C)[O]1[Cu]23Oc4c(OC)cccc4C=[N]2CC[N]3=Cc2cccc(c12)OC.O
• Title of publication: Toward Rational Control of Metal Stoichiometry in Heterobimetallic Coordination Complexes: Synthesis and Characterization of Pb(Hsal)2(Cu(salen*))2, [Pb(NO3)(Cu(salen*))2](NO3), Pb(OAc)2(Cu(salen*)), and [Pb(OAc)(Ni(salen*))2](OAc)
• Authors of publication: John H. Thurston; Christopher G.-Z. Tang; Daniel W. Trahan; Kenton H. Whitmire
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 2708 - 2713
• a: 9.99 ± 0.002 Å
• b: 10.759 ± 0.002 Å
• c: 12.576 ± 0.003 Å
• α: 110.96 ± 0.03°
• β: 103.97 ± 0.03°
• γ: 97.73 ± 0.03°
• Cell volume: 1188 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0218
• Residual factor for significantly intense reflections: 0.0196
• Weighted residual factors for significantly intense reflections: 0.0501
• Weighted residual factors for all reflections included in the refinement: 0.0509
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No