Information card for entry 4310996

Structure parameters

• Formula: C39.5 H60 N4 O2 P2 Si4 U
• Calculated formula: C39.5 H56 N4 O2 P2 Si4 U
• Title of publication: Distorted Equatorial Coordination Environments and Weakening of UO Bonds in Uranyl Complexes Containing NCN and NPN Ligands
• Authors of publication: Mark J. Sarsfield; Madeleine Helliwell; James Raftery
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 3170 - 3179
• a: 16.717 ± 0.004 Å
• b: 13.625 ± 0.003 Å
• c: 21.017 ± 0.005 Å
• α: 90°
• β: 93.519 ± 0.005°
• γ: 90°
• Cell volume: 4778 ± 1.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0522
• Residual factor for significantly intense reflections: 0.0385
• Weighted residual factors for significantly intense reflections: 0.089
• Weighted residual factors for all reflections included in the refinement: 0.096
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No