Information card for entry 4311751

Structure parameters

• Chemical name: bis(hydrotris(3,5-dimethylpyrazolyl)borato)(bis(trimethylsilyl)amido) uranium(III)
• Formula: C46 H82 B2 N13 O2.5 Si2 U
• Calculated formula: C46 H82 B2 N13 O2.5 Si2 U
• Title of publication: Uranium (III) Scorpionates: Synthesis and Structure of [(TpMe2)2U{N(C6H5)2}] and [(TpMe2)2U{N(SiMe3)2}]
• Authors of publication: Maria Augusta Antunes; Gregory M. Ferrence; Ângela Domingos; Robert McDonald; Carol J. Burns; Josef Takats; Noémia Marques
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 6640 - 6643
• a: 10.779 ± 0.002 Å
• b: 16.163 ± 0.003 Å
• c: 16.736 ± 0.003 Å
• α: 82.681 ± 0.004°
• β: 79.948 ± 0.004°
• γ: 71.766 ± 0.004°
• Cell volume: 2718.6 ± 0.9 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0812
• Residual factor for significantly intense reflections: 0.0524
• Weighted residual factors for significantly intense reflections: 0.1083
• Weighted residual factors for all reflections included in the refinement: 0.1249
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No