Crystallography Open Database

Information card for entry 4311754

Preview

Coordinates	4311754.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50.5 H50 F6 N2 O0.5 P3 Rh
Calculated formula	C50.532 H49 F6 N2 O0.532 P3 Rh
Title of publication	Rhodium-Hydrido-Benzylamine-Triphenylphosphine Complexes: Solid-State and Solution Structures and Implications in Catalyzed Imine Hydrogenation
Authors of publication	Paolo Marcazzan; Brian O. Patrick; Brian R. James
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	6838 - 6841
a	29.3124 ± 0.0007 Å
b	21.0184 ± 0.0005 Å
c	18.1676 ± 0.0004 Å
α	90°
β	124.853 ± 0.002°
γ	90°
Cell volume	9185.3 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0622
Residual factor for significantly intense reflections	0.0423
Weighted residual factors for significantly intense reflections	0.1104
Weighted residual factors for all reflections included in the refinement	0.12
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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