Information card for entry 4312003

Structure parameters

• Common name: Ar*PbSi(SiMe3)3.0.5n-hexane
• Formula: C48 H83 Pb Si4
• Calculated formula: C48 H83 Pb Si4
• Title of publication: Terphenyl Ligand Stabilized Lead(II) Derivatives: Steric Effects and Lead-Lead Bonding in Diplumbenes
• Authors of publication: Shirley Hino; Marilyn Olmstead; Andrew D. Phillips; Robert J. Wright; Philip P. Power
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 7346 - 7352
• a: 19.6824 ± 0.0012 Å
• b: 15.91 ± 0.0008 Å
• c: 16.9291 ± 0.001 Å
• α: 90°
• β: 101.041 ± 0.003°
• γ: 90°
• Cell volume: 5203.2 ± 0.5 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0479
• Residual factor for significantly intense reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.0597
• Weighted residual factors for all reflections included in the refinement: 0.0644
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No