Crystallography Open Database

Information card for entry 4312066

4312065 << 4312066 >> 4312067

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Coordinates	4312066.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C106.5 H88.5 O3 Rh3 Sn8
Calculated formula	C106.5 H88.5 O3 Rh3 Sn8
Title of publication	Superloading of Tin Ligands into Rhodium and Iridium Carbonyl Cluster Complexes
Authors of publication	Richard D. Adams; Burjor Captain; Jack L. Smith; Michael B. Hall; Chad L. Beddie; Charles Edwin Webster
Journal of publication	Inorganic Chemistry
Year of publication	2004
Journal volume	43
Pages of publication	7576 - 7578
a	14.3214 ± 0.0008 Å
b	24.7842 ± 0.0013 Å
c	27.6995 ± 0.0015 Å
α	86.43 ± 0.001°
β	87.73 ± 0.001°
γ	89.733 ± 0.001°
Cell volume	9805 ± 0.9 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1498
Residual factor for significantly intense reflections	0.0894
Weighted residual factors for significantly intense reflections	0.2231
Weighted residual factors for all reflections included in the refinement	0.2573
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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