Information card for entry 4312394

Structure parameters

• Formula: C22 H21 Cl5 N2 P2 Pd
• Calculated formula: C22 H21 Cl5 N2 P2 Pd
• Title of publication: Diphosphines Possessing Electronically Different Donor Groups: Synthesis and Coordination Chemistry of the Unsymmetrical Di(N-pyrrolyl)phosphino-Functionalized dppm Analogue Ph2PCH2P(NC4H4)2
• Authors of publication: Andrew D. Burrows; Mary F. Mahon; Steven P. Nolan; Maurizio Varrone
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7227 - 7238
• a: 10.609 ± 0.0002 Å
• b: 17.069 ± 0.0003 Å
• c: 14.552 ± 0.0003 Å
• α: 90°
• β: 96.639 ± 0.0007°
• γ: 90°
• Cell volume: 2617.48 ± 0.09 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0594
• Residual factor for significantly intense reflections: 0.0564
• Weighted residual factors for significantly intense reflections: 0.132
• Weighted residual factors for all reflections included in the refinement: 0.1334
• Goodness-of-fit parameter for all reflections included in the refinement: 1.18
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No