Information card for entry 4312426

Structure parameters

• Formula: C42 H108 Ge2 N4 P2 Pd2 S2 Si8
• Calculated formula: C42 H108 Ge2 N4 P2 Pd2 S2 Si8
• SMILES: c1ccccc1.[Pd]12([P](CC)(CC)CC)[S]3[Ge](N([Si](C)(C)C)[Si](C)(C)C)(N([Si](C)(C)C)[Si](C)(C)C)[Pd]3([P](CC)(CC)CC)[S]1[Ge]2(N([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Reactions of Palladium Germylene Complexes: Formation of Sulfide Bridges
• Authors of publication: Zuzanna T. Cygan; Jeff W. Kampf; Mark M. Banaszak Holl
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7219 - 7226
• a: 11.287 ± 0.0013 Å
• b: 12.7506 ± 0.0015 Å
• c: 13.1569 ± 0.0015 Å
• α: 105.478 ± 0.002°
• β: 112.702 ± 0.002°
• γ: 90.475 ± 0.002°
• Cell volume: 1670.2 ± 0.3 ų
• Cell temperature: 158 ± 2 K
• Ambient diffraction temperature: 158 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0253
• Residual factor for significantly intense reflections: 0.0214
• Weighted residual factors for significantly intense reflections: 0.0544
• Weighted residual factors for all reflections included in the refinement: 0.0566
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No