Information card for entry 4312996

Structure parameters

• Common name: TpOs(N)(ONO2)2
• Formula: C9 H10 B N9 O6 Os
• Calculated formula: C9 H10 B N9 O6 Os
• SMILES: [BH]12n3ccc[n]3[Os]([n]3cccn13)([n]1cccn21)(#N)(ON(=O)=O)ON(=O)=O
• Title of publication: Tuning the Properties of the Osmium Nitrido Group in TpOs(N)X2by Changing the Ancillary Ligand
• Authors of publication: Ahmad Dehestani; Werner Kaminsky; James M. Mayer
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 605 - 611
• a: 7.264 ± 0.008 Å
• b: 13.237 ± 0.011 Å
• c: 16.43 ± 0.02 Å
• α: 90°
• β: 93.26 ± 0.05°
• γ: 90°
• Cell volume: 1577 ± 3 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1875
• Residual factor for significantly intense reflections: 0.0625
• Weighted residual factors for significantly intense reflections: 0.1042
• Weighted residual factors for all reflections included in the refinement: 0.1341
• Goodness-of-fit parameter for all reflections included in the refinement: 0.852
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No