Information card for entry 4313305

Structure parameters

• Formula: C19 H43 Cr F12 N10 Ni O2 P2
• Calculated formula: C19 H39 Cr F12 N10 Ni O2 P2
• Title of publication: High-Nuclearity Metal-Cyanide Clusters: Synthesis, Magnetic Properties, and Inclusion Behavior of Open-Cage Species Incorporating [(tach)M(CN)3] (M = Cr, Fe, Co) Complexes
• Authors of publication: Jenny Y. Yang; Matthew P. Shores; Jennifer J. Sokol; Jeffrey R. Long
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1403 - 1419
• a: 20.832 ± 0.003 Å
• b: 16.324 ± 0.002 Å
• c: 9.734 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3310.2 ± 0.8 ų
• Cell temperature: 155 ± 2 K
• Ambient diffraction temperature: 155 ± 2 K
• Number of distinct elements: 8
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0992
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for all reflections: 0.1984
• Weighted residual factors for significantly intense reflections: 0.1814
• Goodness-of-fit parameter for all reflections: 1.066
• Goodness-of-fit parameter for significantly intense reflections: 1.248
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No