Information card for entry 4313332

Structure parameters

• Common name: [LOEtTi(Cl4cat)]2(mu-O)
• Formula: C46 H70 Cl8 Co2 O23 P6 Ti2
• Calculated formula: C46 H70 Cl8 Co2 O23 P6 Ti2
• Title of publication: Half-Sandwich Titanium(IV) Complexes with Kläui's Tripod Ligand
• Authors of publication: Tony C. H. Lam; Eddie Y. Y. Chan; Wing-Leung Mak; Samuel M. F. Lo; Ian D. Williams; Wing-Tak Wong; Wa-Hung Leung
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1842 - 1847
• a: 10.287 ± 0.003 Å
• b: 13.406 ± 0.003 Å
• c: 14.851 ± 0.004 Å
• α: 69.15 ± 0.01°
• β: 72.42 ± 0.02°
• γ: 70.5 ± 0.01°
• Cell volume: 1764.7 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0909
• Residual factor for significantly intense reflections: 0.0647
• Weighted residual factors for all reflections: 0.2011
• Weighted residual factors for significantly intense reflections: 0.1634
• Goodness-of-fit parameter for all reflections: 1.093
• Goodness-of-fit parameter for significantly intense reflections: 1.147
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No