Information card for entry 4313342

Structure parameters

• Formula: K0.5 Nd2.5 O59.5 Si W11
• Calculated formula: K0.5 Nd2.5 O59.5 Si W11
• Title of publication: Solid-State and Solution Studies of {Lnn(SiW11O39)} Polyoxoanions: An Example of Building Block Condensation Dependent on the Nature of the Rare Earth
• Authors of publication: Pierre Mialane; Laurent Lisnard; Alain Mallard; Jérôme Marrot; Elisabeth Antic-Fidancev; Patrick Aschehoug; Daniel Vivien; Francis Sécheresse
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 2102 - 2108
• a: 12.4824 ± 0.0001 Å
• b: 12.7297 ± 0.0002 Å
• c: 18.6815 ± 0.0001 Å
• α: 86.877 ± 0.001°
• β: 80.152 ± 0.001°
• γ: 82.993 ± 0.001°
• Cell volume: 2901.14 ± 0.05 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0876
• Residual factor for significantly intense reflections: 0.0603
• Weighted residual factors for significantly intense reflections: 0.1404
• Weighted residual factors for all reflections included in the refinement: 0.1511
• Goodness-of-fit parameter for all reflections included in the refinement: 0.908
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No