Information card for entry 4313441

Structure parameters

• Common name: Cu3(dpa)4Cl2SbCl6 2.44(acetone)
• Formula: C47.31 H46.63 Cl8 Cu3 N12 O2.44 Sb
• Calculated formula: C47.32 H46.64 Cl8 Cu3 N12 O2.44 Sb
• Title of publication: Oxidation of Ni3(dpa)4Cl2 and Cu3(dpa)4Cl2: Nickel-Nickel Bonding Interaction, but No Copper-Copper Bonds
• Authors of publication: John F. Berry; F. Albert Cotton; Lee M. Daniels; Carlos A. Murillo; Xiaoping Wang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 2418 - 2427
• a: 15.0331 ± 0.0012 Å
• b: 12.401 ± 0.001 Å
• c: 33.114 ± 0.003 Å
• α: 90°
• β: 99.506 ± 0.003°
• γ: 90°
• Cell volume: 6088.5 ± 0.9 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1457
• Residual factor for significantly intense reflections: 0.1087
• Weighted residual factors for significantly intense reflections: 0.2152
• Weighted residual factors for all reflections included in the refinement: 0.2416
• Goodness-of-fit parameter for all reflections included in the refinement: 1.167
• Method of determination: single crystal
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No