Information card for entry 4313510

Structure parameters

• Formula: C64 H62 Cl4 N8 O2 Pb3 S2
• Calculated formula: C64 H62 Cl4 N8 O2 Pb3 S2
• Title of publication: Compositional and Structural Variety of Diphenyllead(IV) Complexes Obtained by Reaction of Diphenyllead Dichloride with Thiosemicarbazones
• Authors of publication: José S. Casas; Eduardo E. Castellano; J. Ellena; María S. García Tasende; Agustín Sánchez; José Sordo; María J. Vidarte
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 2584 - 2595
• a: 9.83 ± 0.0005 Å
• b: 11.878 ± 0.0006 Å
• c: 14.802 ± 0.0008 Å
• α: 77.33 ± 0.002°
• β: 85.924 ± 0.002°
• γ: 73.693 ± 0.002°
• Cell volume: 1618.29 ± 0.15 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0747
• Residual factor for significantly intense reflections: 0.0545
• Weighted residual factors for significantly intense reflections: 0.1435
• Weighted residual factors for all reflections included in the refinement: 0.16
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No