Information card for entry 4313696

Structure parameters

• Formula: K10 Mo4 O109 P2 S4 W22
• Calculated formula: K10 Mo4 O109 P2 S4 W22
• Title of publication: A Monovacant Heteropolytungstate Thioderivative: Synthesis and Characterization of [(PW~11~O~39~)~2~(H~4~Mo~4~S~4~O~6~)]^10-^ and Related Isomers
• Authors of publication: Jérôme Marrot; Marie Anne Pilette; Francis Sécheresse; Emmanuel Cadot
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 3609 - 3615
• a: 11.6764 ± 0.0001 Å
• b: 13.5414 ± 0.0002 Å
• c: 19.9173 ± 0.0003 Å
• α: 84.302 ± 0.001°
• β: 81.514 ± 0.001°
• γ: 64.484 ± 0.001°
• Cell volume: 2808.69 ± 0.07 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0751
• Residual factor for significantly intense reflections: 0.0599
• Weighted residual factors for significantly intense reflections: 0.1524
• Weighted residual factors for all reflections included in the refinement: 0.1604
• Goodness-of-fit parameter for all reflections included in the refinement: 0.969
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No