Information card for entry 4313707

Structure parameters

• Formula: C39 H28 Cl4 F10 N4 O3 Pd2
• Calculated formula: C39 H28 Cl4 F10 N4 O3 Pd2
• Title of publication: Insertion Reactions into Pd-O and Pd-N Bonds: Preparation of Alkoxycarbonyl, Carbonato, Carbamato, Thiocarbamate, and Thioureide Complexes of Palladium(II)
• Authors of publication: José Ruiz; M. Teresa Martínez; Félix Florenciano; Venancio Rodríguez; Gregorio López; José Pérez; Penny A. Chaloner; Peter B. Hitchcock
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 3650 - 3661
• a: 11.1311 ± 0.0006 Å
• b: 11.6741 ± 0.0007 Å
• c: 17.0116 ± 0.0008 Å
• α: 70.81 ± 0.004°
• β: 84.557 ± 0.004°
• γ: 84.114 ± 0.004°
• Cell volume: 2072.3 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0427
• Residual factor for significantly intense reflections: 0.0323
• Weighted residual factors for significantly intense reflections: 0.0829
• Weighted residual factors for all reflections included in the refinement: 0.0873
• Goodness-of-fit parameter for all reflections included in the refinement: 0.869
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No