Information card for entry 4313901

Structure parameters

• Formula: C43 H60 B N8 P Pt S3 W
• Calculated formula: C43 H60 B N8 P Pt S3 W
• Title of publication: Cubane-Type Heterometallic Sulfido Clusters: Incorporation of Two Metal Fragments into a Dinuclear ReS(μ-S)2ReS Core Affording Bimetallic M2Re2(μ3-S)4 Clusters (M = Ru, Pt, Cu) or Trimetallic MM'Re2(μ3-S)4 Clusters via Incomplete Cubane-Type MRe2(μ3-S)(μ2-S)3 Intermediates (M = Ru, Rh, Ir; M' = Mo, W, Pd, Ru, Rh)
• Authors of publication: Seino, Hidetake; Kaneko, Tetsuhide; Fujii, Shunpei; Hidai, Masanobu; Mizobe, Yasushi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Journal issue: 15
• Pages of publication: 4585 - 4596
• a: 10.94 ± 0.001 Å
• b: 17.208 ± 0.003 Å
• c: 25.248 ± 0.001 Å
• α: 90°
• β: 97.449 ± 0.008°
• γ: 90°
• Cell volume: 4713 ± 1 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0366
• Residual factor for significantly intense reflections: 0.0366
• Weighted residual factors for significantly intense reflections: 0.0375
• Weighted residual factors for all reflections included in the refinement: 0.0375
• Goodness-of-fit parameter for all reflections included in the refinement: 1.304
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No