Information card for entry 4314019

Structure parameters

• Formula: C31 H46 N0.33 O3 P
• Calculated formula: C31 H46 N0.333333 O3 P
• Title of publication: Sterically Congested Tripodal Phosphites: Conformational Analysis, Solid-State Polymorphism, Metal Complexation, and Application to the Asymmetric Hydrosilation of Ketones1
• Authors of publication: Sai P. Shum; Stephen D. Pastor; Anthony D. DeBellis; Paul A. Odorisio; Lilibeth Burke; Frank H. Clarke; Grety Rihs; Bogdan Piatek; Ronald K. Rodebaugh
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 5097 - 5106
• a: 25.991 ± 0.003 Å
• b: 25.991 ± 0.003 Å
• c: 24.649 ± 0.003 Å
• α: 90 ± 0.01°
• β: 90 ± 0.01°
• γ: 120 ± 0.01°
• Cell volume: 14420 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 146
• Hermann-Mauguin space group symbol: R 3 :H
• Hall space group symbol: R 3
• Residual factor for all reflections: 0.1221
• Residual factor for significantly intense reflections: 0.0721
• Weighted residual factors for all reflections: 0.1963
• Weighted residual factors for significantly intense reflections: 0.1621
• Goodness-of-fit parameter for all reflections: 1.258
• Goodness-of-fit parameter for significantly intense reflections: 1.282
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No