Information card for entry 4314076

Structure parameters

• Formula: C23.14 H45.43 B0.86 Co0.86 I0.86 P2.57
• Calculated formula: C23.1429 H45.4286 B0.857143 Co0.857143 I0.857143 P2.57143
• Title of publication: The Strong-Field Tripodal Phosphine Donor, [PhB(CH2PiPr2)3]-, Provides Access to Electronically and Coordinatively Unsaturated Transition Metal Complexes
• Authors of publication: Theodore A. Betley; Jonas C. Peters
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 5074 - 5084
• a: 46.165 ± 0.003 Å
• b: 12.234 ± 0.0008 Å
• c: 34.353 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 19402 ± 2 ų
• Cell temperature: 96 ± 2 K
• Ambient diffraction temperature: 96 ± 2 K
• Number of distinct elements: 6
• Space group number: 64
• Hermann-Mauguin space group symbol: C m c a
• Hall space group symbol: -C 2ac 2
• Residual factor for all reflections: 0.1537
• Residual factor for significantly intense reflections: 0.0602
• Weighted residual factors for significantly intense reflections: 0.1217
• Weighted residual factors for all reflections included in the refinement: 0.1436
• Goodness-of-fit parameter for all reflections included in the refinement: 1.367
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No