Information card for entry 4314159

Structure parameters

• Formula: Cs8 H38 Nb6 O96 Si2 W18
• Calculated formula: Cs7.958 Nb6 O96 Si2 W18
• Title of publication: Dimerization of A-α-[SiNb3W9O40]7- by pH-Controlled Formation of Individual Nb-μ-O-Nb Linkages
• Authors of publication: Gyu-Shik Kim; Huadong Zeng; Wade A. Neiwert; Jennifer J. Cowan; Donald VanDerveer; Craig L. Hill; Ira A. Weinstock
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 5537 - 5544
• a: 40.847 ± 0.002 Å
• b: 13.213 ± 0.0007 Å
• c: 16.8179 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9076.8 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 63
• Hermann-Mauguin space group symbol: C m c m
• Hall space group symbol: -C 2c 2
• Residual factor for all reflections: 0.1353
• Residual factor for significantly intense reflections: 0.0685
• Weighted residual factors for all reflections: 0.1647
• Weighted residual factors for all reflections included in the refinement: 0.1407
• Goodness-of-fit parameter for all reflections: 1.023
• Goodness-of-fit parameter for all reflections included in the refinement: 1.155
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No