Information card for entry 4314441

Structure parameters

• Formula: C260 H268 Ag14 O11 P8 Se13
• Calculated formula: C256 H260 Ag14 O11 P8 Se13
• Title of publication: Presence or Absence of a Central Se Atom in Silver Selenide/Selenolate Clusters with Halite Topology: Syntheses and Properties of [(Ph3PAg)8Ag6(μ6-Se)1-x/2(SePh)12]x+ (x= 0, 1)
• Authors of publication: Hari Pada Nayek; Werner Massa; Stefanie Dehnen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 144 - 149
• a: 31.7987 ± 0.0009 Å
• b: 22.9837 ± 0.0004 Å
• c: 33.2185 ± 0.0008 Å
• α: 90°
• β: 92.257 ± 0.002°
• γ: 90°
• Cell volume: 24259 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2193
• Residual factor for significantly intense reflections: 0.0743
• Weighted residual factors for significantly intense reflections: 0.1252
• Weighted residual factors for all reflections included in the refinement: 0.1625
• Goodness-of-fit parameter for all reflections included in the refinement: 0.749
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No