Information card for entry 4314566

Structure parameters

• Chemical name: (K-crypt)3[GeSn8-CHCH2] 1en 1tol
• Formula: C61.5 H123 Ge K3 N8 O18 Sn8
• Calculated formula: C61.5 H123 Ge K3 N8 O18 Sn8
• Title of publication: Heteroatomic Deltahedral Zintl Ions of Group 14 and their Alkenylation
• Authors of publication: Miriam M. Gillett-Kunnath; Ivaylo Petrov; Slavi C. Sevov
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 721 - 729
• a: 13.922 ± 0.0003 Å
• b: 14.9788 ± 0.0003 Å
• c: 21.5892 ± 0.0005 Å
• α: 94.258 ± 0.001°
• β: 98.521 ± 0.001°
• γ: 98.489 ± 0.001°
• Cell volume: 4382.31 ± 0.17 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0561
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.0904
• Weighted residual factors for all reflections included in the refinement: 0.0984
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No