Information card for entry 4314569

Structure parameters

• Chemical name: (K-crypt)3[Ge2Sn7-CHCHPh] 2en
• Formula: C66 H131 Ge2 K3 N10 O18 Sn7
• Calculated formula: C66 H131 Ge2 K3 N10 O18 Sn7
• Title of publication: Heteroatomic Deltahedral Zintl Ions of Group 14 and their Alkenylation
• Authors of publication: Miriam M. Gillett-Kunnath; Ivaylo Petrov; Slavi C. Sevov
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 721 - 729
• a: 13.2583 ± 0.0005 Å
• b: 47.0565 ± 0.0017 Å
• c: 15.9978 ± 0.0006 Å
• α: 90°
• β: 111.536 ± 0.002°
• γ: 90°
• Cell volume: 9284.1 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0896
• Residual factor for significantly intense reflections: 0.0737
• Weighted residual factors for significantly intense reflections: 0.184
• Weighted residual factors for all reflections included in the refinement: 0.1963
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No