Information card for entry 4314574

Structure parameters

• Chemical name: tetrakis(Tris(4-pyridylmethyl)cyclotriguaiacylene)trispalladium nitrate
• Formula: C184 H209 N15 O43.5 Pd8 S3
• Calculated formula: C184 H198 N15 O43.5 Pd3 S8
• Title of publication: Tripodal 4-Pyridyl-Derived Host Ligands and Their Metallo-Supramolecular Chemistry: Stella Octangula and Bowl-Shaped Assemblies
• Authors of publication: Tanya K. Ronson; Christopher Carruthers; Julie Fisher; Thierry Brotin; Lindsay P. Harding; Pierre J. Rizkallah; Michaele J. Hardie
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 675 - 685
• a: 43.49 ± 0.03 Å
• b: 28.1 ± 0.03 Å
• c: 40.83 ± 0.04 Å
• α: 90°
• β: 100.545 ± 0.015°
• γ: 90°
• Cell volume: 49054 ± 8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1491
• Residual factor for significantly intense reflections: 0.1122
• Weighted residual factors for significantly intense reflections: 0.3009
• Weighted residual factors for all reflections included in the refinement: 0.3267
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation type: synchrotron,l=0.7977
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No