Information card for entry 4315065

Structure parameters

• Formula: C58 H95 B Cl2 Li N2 O7 Pr
• Calculated formula: C58 H95 B Cl2 Li N2 O7 Pr
• Title of publication: Lanthanide Complexes of Boraamidinate Ligands: Synthesis and X-ray Structures of {[Li(THF)4][bamLnCl2(THF)]}2 (bam= [PhB(NDipp)2]2-; Ln = Y, Pr, Nd, Sm, Ho, Er, Yb) and {bamLnCl(THF)2}2 (Ln = Y, Sm)
• Authors of publication: Andrea M. Corrente; Tristram Chivers
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 2457 - 2463
• a: 13.32 ± 0.003 Å
• b: 21.595 ± 0.004 Å
• c: 22.19 ± 0.004 Å
• α: 90°
• β: 103.04 ± 0.03°
• γ: 90°
• Cell volume: 6218 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0887
• Residual factor for significantly intense reflections: 0.062
• Weighted residual factors for significantly intense reflections: 0.1182
• Weighted residual factors for all reflections included in the refinement: 0.1296
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No