Information card for entry 4315080

Structure parameters

• Chemical name: Tetradecacyclopentyl-bis(silsesquioxane)-tri(oxovanadium) bis(tetrahydrofuran)-adduct
• Formula: C78 H142 O29 Si14 V3
• Calculated formula: C78 H142 O29 Si14 V3
• Title of publication: Oxovanadium(IV) Silsesquioxane Complexes
• Authors of publication: Christian Ohde; Christian Limberg; Reinhard Stösser; Serhiy Demeshko
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 2479 - 2485
• a: 25.9729 ± 0.0005 Å
• b: 19.574 ± 0.0004 Å
• c: 20.5865 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10466 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.1173
• Residual factor for significantly intense reflections: 0.1052
• Weighted residual factors for significantly intense reflections: 0.2268
• Weighted residual factors for all reflections included in the refinement: 0.2309
• Goodness-of-fit parameter for all reflections included in the refinement: 1.266
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No