Information card for entry 4315308

Structure parameters

• Formula: C37 H107 N6 O Si12 U3
• Calculated formula: C37 H107 N6 O Si12 U3
• SMILES: [U]123([O](C)[U]45([CH]16[U](N([Si](C)(C)C)[Si]6(C)C)(N([Si](C)(C)C)[Si](C)(C)C)([CH2]3[Si](N2[Si](C)(C)C)(C)C)[CH2]4[Si](N5[Si](C)(C)C)(C)C)[N]([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Ligand Metalation in the Reactivity of a Tetravalent Uranium Amides
• Authors of publication: Ilia Korobkov; Sandro Gambarotta
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 3409 - 3418
• a: 11.923 ± 0.003 Å
• b: 13.947 ± 0.004 Å
• c: 22.855 ± 0.006 Å
• α: 79.887 ± 0.006°
• β: 75.655 ± 0.005°
• γ: 67.832 ± 0.005°
• Cell volume: 3395.6 ± 1.6 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1664
• Residual factor for significantly intense reflections: 0.0668
• Weighted residual factors for significantly intense reflections: 0.0797
• Weighted residual factors for all reflections included in the refinement: 0.0985
• Goodness-of-fit parameter for all reflections included in the refinement: 0.934
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No