Information card for entry 4315337

Structure parameters

• Formula: C33 H60 B2 P2
• Calculated formula: C33 H60 B2 P2
• SMILES: [PH]([BH3])(CCC[PH]([BH3])c1c(C(C)C)cc(C(C)C)cc1C(C)C)c1c(C(C)C)cc(C(C)C)cc1C(C)C
• Title of publication: Synthesis of Gold Phosphido Complexes Derived from Bis(secondary) Phosphines. Structure of Tetrameric [Au(MesP(CH2)3PMes)Au]4
• Authors of publication: Elizabeth M. Lane; Timothy W. Chapp; Russell P. Hughes; David S. Glueck; Brett C. Feland; Guy M. Bernard; Roderick E. Wasylishen; Arnold L. Rheingold
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 3950 - 3957
• a: 9.204 ± 0.0012 Å
• b: 33.389 ± 0.004 Å
• c: 12.161 ± 0.0016 Å
• α: 90°
• β: 109.068 ± 0.002°
• γ: 90°
• Cell volume: 3532.2 ± 0.8 ų
• Cell temperature: 208 ± 2 K
• Ambient diffraction temperature: 208 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0866
• Residual factor for significantly intense reflections: 0.0588
• Weighted residual factors for significantly intense reflections: 0.1353
• Weighted residual factors for all reflections included in the refinement: 0.1548
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No