Information card for entry 4315347

Structure parameters

• Common name: SiP3(dmpe)FeClCl
• Formula: C16 H43 Cl2 Fe P5 Si
• Calculated formula: C16 H43 Cl2 Fe P5 Si
• Title of publication: Synthesis and Characterization of Pentaphosphino Zero-Valent Iron Complexes and Their Corresponding Iron(II)-Chloride and -Hydride Complexes
• Authors of publication: Kristen A. Thoreson; Angela D. Follett; Kristopher McNeill
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 3942 - 3949
• a: 33.776 ± 0.002 Å
• b: 9.5076 ± 0.0007 Å
• c: 18.121 ± 0.001 Å
• α: 90°
• β: 115.254 ± 0.001°
• γ: 90°
• Cell volume: 5263 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0429
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.068
• Weighted residual factors for all reflections included in the refinement: 0.0721
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No