Information card for entry 4315350

Structure parameters

• Common name: (dmpe)5Fe2
• Formula: C15 H40 Fe P5
• Calculated formula: C15 H40 Fe P5
• Title of publication: Synthesis and Characterization of Pentaphosphino Zero-Valent Iron Complexes and Their Corresponding Iron(II)-Chloride and -Hydride Complexes
• Authors of publication: Kristen A. Thoreson; Angela D. Follett; Kristopher McNeill
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 3942 - 3949
• a: 9.075 ± 0.001 Å
• b: 9.224 ± 0.001 Å
• c: 15.328 ± 0.002 Å
• α: 101.02 ± 0.002°
• β: 98.323 ± 0.002°
• γ: 113.373 ± 0.002°
• Cell volume: 1120.9 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0447
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0696
• Weighted residual factors for all reflections included in the refinement: 0.0756
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No