Information card for entry 4315667

Structure parameters

• Common name: F3 O2 Os N C2 H3 2(C2 H3 N)
• Formula: C6 H9 F2 N3 O3 Os
• Calculated formula: C6 H9 F2 N3 O3 Os
• Title of publication: Syntheses and Multi-NMR Study of fac- and mer-OsO3F2(NCCH3) and the X-ray Crystal Structure (n= 2) and Raman Spectrum (n= 0) of fac-OsO3F2(NCCH3).nCH3CN
• Authors of publication: Michael J. Hughes; Michael Gerken; Hélène P. A. Mercier; Gary J. Schrobilgen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 4768 - 4780
• a: 7.7995 ± 0.0002 Å
• b: 14.7327 ± 0.0004 Å
• c: 9.521 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1094.04 ± 0.05 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0215
• Residual factor for significantly intense reflections: 0.0178
• Weighted residual factors for significantly intense reflections: 0.0403
• Weighted residual factors for all reflections included in the refinement: 0.0413
• Goodness-of-fit parameter for all reflections included in the refinement: 1.097
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No