Information card for entry 4315832

Structure parameters

• Formula: H62 N12 Ni6 O40 S5
• Calculated formula: H50 N12 Ni6 O40 S5
• Title of publication: Novel Polynuclear Nickel(II) Complex: Hydrazine, Sulfato, and Hydroxo Bridging in an Unusual Metal Hexamer. Crystal Structure and Magnetic Properties of [Ni6(N2H4)6(SO4)4(OH)2(H2O)8](SO4)(H2O)10
• Authors of publication: Magnus Gustafsson; Andreas Fischer; Andrey Ilyukhin; Mikhail Maliarik; Per Nordblad
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 5359 - 5361
• a: 10.965 ± 0.002 Å
• b: 11.214 ± 0.003 Å
• c: 11.306 ± 0.003 Å
• α: 60.19 ± 0.02°
• β: 71.96 ± 0.02°
• γ: 69.23 ± 0.02°
• Cell volume: 1112.5 ± 0.5 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0595
• Residual factor for significantly intense reflections: 0.0489
• Weighted residual factors for significantly intense reflections: 0.1428
• Weighted residual factors for all reflections included in the refinement: 0.1504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No