Information card for entry 4316178

Structure parameters

• Formula: C21 H5 Bi O15 Os4
• Calculated formula: C21 H5 Bi O15 Os4
• SMILES: [Os]1([Os]([Bi]21[Os]([Os]2(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])C#[O])(c1ccccc1)(C#[O])(C#[O])C#[O]
• Title of publication: Osmium-Bismuth Complexes from the Reaction of Os3(CO)11(NCMe) with BiPh3
• Authors of publication: Richard D. Adams; William C. Pearl
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 7170 - 7175
• a: 10.8919 ± 0.0004 Å
• b: 17.0759 ± 0.0006 Å
• c: 16.1745 ± 0.0006 Å
• α: 90°
• β: 103.305 ± 0.001°
• γ: 90°
• Cell volume: 2927.53 ± 0.18 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0478
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0613
• Weighted residual factors for all reflections included in the refinement: 0.0674
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No