Information card for entry 4316455

Structure parameters

• Formula: C22 H60 N3 Na O Si6 U
• Calculated formula: C22 H60 N3 Na O Si6 U
• SMILES: C[Si](C)(C)N1[U]2(C[Si](C)(C)[N]2[Si](C)(C)C)(N([Si](C)(C)C)[Si](C)(C)C)C[Si]1(C)C.[Na+].O1CCCC1
• Title of publication: The Bis Metallacyclic Anion [U(N{SiMe3}2)(CH2SiMe2N{SiMe3})2]-
• Authors of publication: Olivier Bénaud; Jean-Claude Berthet; Pierre Thuéry; Michel Ephritikhine
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 8117 - 8130
• a: 8.5677 ± 0.0006 Å
• b: 40.256 ± 0.005 Å
• c: 22.157 ± 0.003 Å
• α: 90°
• β: 92.334 ± 0.007°
• γ: 90°
• Cell volume: 7635.6 ± 1.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1554
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.064
• Weighted residual factors for all reflections included in the refinement: 0.0764
• Goodness-of-fit parameter for all reflections included in the refinement: 0.894
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No