Information card for entry 4316485

Structure parameters

• Formula: C144 H124 Au8 O44 P8 Si W12
• Calculated formula: C144 H120 Au8 O44 P8 Si W12
• Title of publication: Intercluster Compound between a Tetrakis{triphenylphosphinegold(I)}oxonium Cation and a Keggin Polyoxometalate (POM): Formation during the Course of Carboxylate Elimination of a Monomeric Triphenylphosphinegold(I) Carboxylate in the Presence of POMs
• Authors of publication: Kenji Nomiya; Takuya Yoshida; Yoshitaka Sakai; Arisa Nanba; Shinichiro Tsuruta
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 8247 - 8254
• a: 28.606 ± 0.0016 Å
• b: 19.0414 ± 0.0016 Å
• c: 32.434 ± 0.002 Å
• α: 90°
• β: 107.659 ± 0.002°
• γ: 90°
• Cell volume: 16834 ± 2 ų
• Cell temperature: 90 K
• Ambient diffraction temperature: 90 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.0549
• Weighted residual factors for significantly intense reflections: 0.1386
• Weighted residual factors for all reflections included in the refinement: 0.1476
• Goodness-of-fit parameter for all reflections included in the refinement: 1.159
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No