Information card for entry 4316534

Structure parameters

• Formula: C20 H20 La4 O32 S4 W4
• Calculated formula: C20 H12 La4 O32 S4 W4
• Title of publication: Synthesis and Structure of Pillared Molybdates and Tungstates with Framework Layers
• Authors of publication: Jennifer L. Nicholls; Sarah E. Hulse; Samantha K. Callear; Graham J. Tizzard; Richard A. Stephenson; Michael B. Hursthouse; William Clegg; Ross W. Harrington; Andrew M. Fogg
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 8545 - 8551
• a: 7.255 ± 0.0002 Å
• b: 8.111 ± 0.0002 Å
• c: 16.931 ± 0.0004 Å
• α: 80.408 ± 0.001°
• β: 78.681 ± 0.001°
• γ: 89.674 ± 0.001°
• Cell volume: 962.9 ± 0.04 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0483
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for significantly intense reflections: 0.0779
• Weighted residual factors for all reflections included in the refinement: 0.0827
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No