Information card for entry 4317738

Structure parameters

• Formula: C38 H33 Cl2 N2 P2 Re S2
• Calculated formula: C38 Cl2 N1.98 P2 Re S2
• Title of publication: Chelated Hydrazido(3-)rhenium(V) Complexes: On the Way to the Nitrido-M(V) Core (M = Tc, Re)
• Authors of publication: Franck Mévellec; Nicolas Lepareur; Alain Roucoux; Nicolas Noiret; Henri Patin; Giuliano Bandoli; Marina Porchia; Francesco Tisato
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 1591 - 1597
• a: 17.514 ± 0.004 Å
• b: 10.639 ± 0.002 Å
• c: 20.106 ± 0.004 Å
• α: 90°
• β: 102.29 ± 0.03°
• γ: 90°
• Cell volume: 3660.5 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0456
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.1137
• Weighted residual factors for all reflections included in the refinement: 0.1147
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No