Information card for entry 4317781

Structure parameters

• Formula: C84 H84 As4 Cu2 F12 P6
• Calculated formula: C83.996 H79 As4 Cu2 F12 P6
• Title of publication: Synthesis and Resolution of (R*,R*)-(\±)-1,1,4,7,10,10-Hexaphenyl-1,10-diarsa-4,7-diphosphadecane: New Ligand for the Stereoselective Self-Assembly of Dicopper(I), Disilver(I), and Digold(I) Helicates
• Authors of publication: Vernon C. Cook; Anthony C. Willis; Johann Zank; S. Bruce Wild
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 1897 - 1906
• a: 16.084 ± 0.003 Å
• b: 18.376 ± 0.003 Å
• c: 29.149 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8615 ± 3 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0829
• Residual factor for significantly intense reflections: 0.0446
• Weighted residual factors for all reflections: 0.0593
• Weighted residual factors for all reflections included in the refinement: 0.0536
• Goodness-of-fit parameter for all reflections: 1.485
• Goodness-of-fit parameter for all reflections included in the refinement: 1.659
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No