Information card for entry 4317797

Structure parameters

• Formula: C22 H25 Au B Cl4 N9 O4
• Calculated formula: C22 H25 Au B Cl4 N9 O4
• Title of publication: Synthesis of Tris- and Tetrakis(pyrazol-1-yl)borate Gold(III) Complexes. Crystal Structures of [Au{κ2-N,N'-BH(Pz)3}Cl2] (pz = Pyrazol-1-yl) and [Au{κ2-N,N'-B(Pz)4}(κ2-C,N-C6H4CH2NMe2-2)]ClO4.CHCl3
• Authors of publication: José Vicente; María Teresa Chicote; Rita Guerrero; Ulrich Herber; Delia Bautista
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 1870 - 1875
• a: 8.5602 ± 0.0009 Å
• b: 16.1203 ± 0.0018 Å
• c: 21.792 ± 0.0019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3007.1 ± 0.5 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0738
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.1022
• Weighted residual factors for all reflections included in the refinement: 0.114
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No