Metal Complexes of Tetrapodal Ligands: Synthesis, Spectroscopic and Thermal Studies, and X-ray Crystal Structure Studies of Na(I), Ca(II), Sr(II), and Ba(II) Complexes of Tetrapodal Ligands N,N,N',N'-Tetrakis(2-hydroxypropyl)ethylenediamine and N,N,N',N'-Tetrakis(2-hydroxyethyl)ethylenediamine
Authors of publication
Geeta Hundal; Maninder Singh Hundal; Sangeeta Obrai; N. S. Poonia; Subodh Kumar
Journal of publication
Inorganic Chemistry
Year of publication
2002
Journal volume
41
Pages of publication
2077 - 2086
a
12.12 ± 0.002 Å
b
14.253 ± 0.003 Å
c
18.677 ± 0.004 Å
α
90°
β
104.67 ± 0.03°
γ
90°
Cell volume
3121.2 ± 1.2 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0617
Residual factor for significantly intense reflections
0.0436
Weighted residual factors for all reflections
0.2265
Weighted residual factors for significantly intense reflections
0.1059
Goodness-of-fit parameter for all reflections
1.055
Goodness-of-fit parameter for significantly intense reflections
