Crystallography Open Database

Information card for entry 4317931

Preview

Coordinates	4317931.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	compound 3
Formula	C53.25 H48 Al6 F18 N6
Calculated formula	C53.25 H48 Al6 F18 N6
Title of publication	Reactions of AlH3.NMe3 with Nitriles: Structural Characterization and Substitution Reactions of Hexameric Aluminum Imides
Authors of publication	N. Dastagiri Reddy; Herbert W. Roesky; Mathias Noltemeyer; Hans-Georg Schmidt
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	2374 - 2378
a	17.527 ± 0.011 Å
b	18.894 ± 0.012 Å
c	19.246 ± 0.015 Å
α	96.11 ± 0.07°
β	102.23 ± 0.04°
γ	106.79 ± 0.03°
Cell volume	5867 ± 7 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1637
Residual factor for significantly intense reflections	0.1125
Weighted residual factors for significantly intense reflections	0.3108
Weighted residual factors for all reflections included in the refinement	0.3831
Goodness-of-fit parameter for all reflections included in the refinement	1.429
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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