Information card for entry 4318016

Structure parameters

• Formula: C15 H15 As N3 O9 V2
• Calculated formula: C15 H15 As N3 O9 V2
• Title of publication: Novel Vanadium(V) Compounds with a Layer Structure: Synthesis, Crystal Structures, and Solid State NMR Spectroscopy of [(VO2)2(4,4'-bpy)0.5(4,4'-Hbpy)(XO4)].H2O (X = P and As)
• Authors of publication: Li-Hsun Huang; Hsien-Ming Kao; Kwang-Hwa Lii
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 2936 - 2940
• a: 7.8843 ± 0.0006 Å
• b: 10.3686 ± 0.0007 Å
• c: 12.2606 ± 0.0009 Å
• α: 113.464 ± 0.001°
• β: 95.56 ± 0.001°
• γ: 94.585 ± 0.001°
• Cell volume: 907.35 ± 0.11 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0279
• Residual factor for significantly intense reflections: 0.0245
• Weighted residual factors for significantly intense reflections: 0.0677
• Weighted residual factors for all reflections included in the refinement: 0.0691
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No