Crystallography Open Database

Information card for entry 4318061

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Coordinates	4318061.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66.5 H68 Cl2 P4 Pt2 S3
Calculated formula	C66.5 H68 Cl2 P4 Pt2 S3
Title of publication	Diverse Evolution of [{Ph2P(CH2)nPPh2}Pt(μ-S)2Pt{Ph2P(CH2)nPPh2}] (n= 2, 3) Metalloligands in CH2Cl2
Authors of publication	Rubén Mas-Ballesté; Mercè Capdevila; Paul A. Champkin; William Clegg; Robert A. Coxall; Agustí Lledós; Claire Mégret; Pilar González-Duarte
Journal of publication	Inorganic Chemistry
Year of publication	2002
Journal volume	41
Pages of publication	3218 - 3229
a	13.8539 ± 0.0005 Å
b	13.0377 ± 0.0005 Å
c	34.1386 ± 0.0013 Å
α	90°
β	91.7764 ± 0.0006°
γ	90°
Cell volume	6163.3 ± 0.4 Å³
Cell temperature	160 ± 2 K
Ambient diffraction temperature	160 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0706
Residual factor for significantly intense reflections	0.0464
Weighted residual factors for significantly intense reflections	0.0914
Weighted residual factors for all reflections included in the refinement	0.0982
Goodness-of-fit parameter for all reflections included in the refinement	1.068
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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