Information card for entry 4318144

Structure parameters

• Formula: C64 H88 Cl3 La N16 O24
• Calculated formula: C64 H68 Cl3 La N16 O24
• Title of publication: Synthesis, Structures, and Magnetic Properties of a Series of Lanthanum(III) and Gadolinium(III) Complexes with Chelating Benzimidazole-Substituted Nitronyl Nitroxide Free Radicals. Evidence for Antiferromagnetic GdIII-Radical Interactions
• Authors of publication: Christophe Lescop; Elie Belorizky; Dominique Luneau; Paul Rey
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 3375 - 3384
• a: 11.0682 ± 0.0008 Å
• b: 34.24 ± 0.003 Å
• c: 42.787 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 16215 ± 2 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 6
• Space group number: 70
• Hermann-Mauguin space group symbol: F d d d :1
• Hall space group symbol: F 2 2 -1d
• Residual factor for all reflections: 0.0965
• Residual factor for significantly intense reflections: 0.0876
• Weighted residual factors for significantly intense reflections: 0.2281
• Weighted residual factors for all reflections included in the refinement: 0.2336
• Goodness-of-fit parameter for all reflections included in the refinement: 1.995
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No