Information card for entry 4318169

Structure parameters

• Formula: C38.5 H53 F10 O6.63 S11 Yb4
• Calculated formula: C38.52 H53.04 F10 O6.63 S11 Yb4
• Title of publication: Chalcogen-Rich Lanthanide Clusters with Fluorinated Thiolate Ligands
• Authors of publication: Mark Fitzgerald; Thomas J. Emge; John G. Brennan
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 3528 - 3532
• a: 12.252 ± 0.002 Å
• b: 17.763 ± 0.006 Å
• c: 27.199 ± 0.005 Å
• α: 90 ± 0.02°
• β: 91.52 ± 0.02°
• γ: 90 ± 0.02°
• Cell volume: 5917 ± 2 ų
• Cell temperature: 153 ± 5 K
• Ambient diffraction temperature: 153 ± 5 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0902
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for significantly intense reflections: 0.1371
• Weighted residual factors for all reflections included in the refinement: 0.147
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No