Information card for entry 4318171

Structure parameters

• Common name: (2,2'-bipyridyl)(tris(3-phenylpyrazolyl)borate)copper(II)perchlorate methylene chloride.monohydrate
• Formula: C38 H34 B Cl3 Cu N8 O5
• Calculated formula: C38 H30 B Cl3 Cu N8 O5
• Title of publication: Effect of Steric Encumbrance of Tris(3-phenylpyrazolyl)borate on the Structure and Properties of Ternary Copper(II) Complexes Having N,N-Donor Heterocyclic Bases
• Authors of publication: Shanta Dhar; Pattubala A. N. Reddy; Munirathinam Nethaji; Subramony Mahadevan; Manas K. Saha; Akhil R. Chakravarty
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 3469 - 3476
• a: 11.111 ± 0.007 Å
• b: 30.197 ± 0.005 Å
• c: 11.527 ± 0.003 Å
• α: 90°
• β: 94.42 ± 0.03°
• γ: 90°
• Cell volume: 3856 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1269
• Residual factor for significantly intense reflections: 0.0736
• Weighted residual factors for significantly intense reflections: 0.1892
• Weighted residual factors for all reflections included in the refinement: 0.2185
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No